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Georges Friedel Laboratory


 
The Georges Friedel Laboratory - LGF (CNRS UMR 5307) is a joint research unit from INSIS-CNRS and École des Mines de Saint-Étienne, comprising 150 persons, dealing with activities in the fields of Materials Science, Mechanics and Process Engineering.
LGF is an academic research player, in strong partnership with industry, addressing the durability and energy efficiency of components, from grain to material, from material to component and from component to factory.
Research at LGF focuses on materials for application in the main fields of energy, transportation, chemistry. Competences are material science, physico-chemistry of solids (divided and massive), mechanics and chemical engineering.
Scientists at LGF develop multiscale models from nano to macroscale, technological solutions for enriching knowledge and design of materials and processes with regard to their functional properties.

  • LGF_PDMM Pin-on-disk tribometer
    Pin-on-disk tribometer coupled with image acquisition © BOUCHOT-DESCARTES-GAVET-PINOLI_LTDS-LGF
    LGF_PDMM Pin-on-disk tribometer
  • LGF_PDMM_Third-body particles observed after a dry friction
    Third-body particles observed after a dry friction © BOUCHOT-DESCARTES-GAVET-PINOLI_LTDS-LGF
    LGF_PDMM_Third-body particles observed after a dry friction
  • LGF_PMM fs laser peening
    Ultrafast laser peening of 2024-T351 aluminium alloy – effect of process parameters on surface topography and microstructure © Nakhoul_LGF
    LGF_PMM fs laser peening
  • LGF_SURF Pre-oxidized Zy4 plate
    Pre-oxidized Zy4 plate © Gestin_LGF
    LGF_SURF Pre-oxidized Zy4 plate
  • LGF_SURF_Local detection of hydrogen at the surface of materials using Kelvin probe (SKPFM)
    Local detection of hydrogen at the surface of materials using Kelvin probe (SKPFM) © Tohme_LGF
    LGF_SURF_Local detection of hydrogen at the surface of materials using Kelvin probe (SKPFM)
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NATIONAL AND INTERNATIONAL COLLABORATIONS AND NETWORKS
LGF participates in numerous federative structures or research groups:
  • The IngéLySe federation (Lyon /Saint-Etienne Engineering research Federation, FR CNRS 3411);
  • More than 10 CNRS Research groups (GDR) dealing with material science, design, engineering;
  • The Laboratory of Excellence – LabEx Manutech-SISE;
  • The Manutech-SLEIGHT Graduate School;
  • CLYM, the Consortium Lyon Saint-Etienne of Microscopy;
  • AXELERA and CIMES, two regional competitiveness clusters.
 
 


RESEARCH TEAMS INVOLVED IN THE MANUTEH-SLEIGHT GRADUATE SCHOOL

Three of the four LGF's research groups are involved in Manutech-SLEIGHT Graduate School.
 

PHYSICS AND MECHANICS OF MATERIALS - PMM

The PMM group works on microstructural evolutions and thermomechanical processing from alloy design to in-service mechanical properties. They develop cutting-edge characterization methods to measure process signatures in terms of microstructure, texture, dislocation density, mechanical properties, damage or residual stresses. In parallel, the PMM group is involved in the development of mean/full field models in the framework of computational mechanics and metallurgy. Recent advances in alloy design and elaboration places the PMM group as one of the main actor in the field of High Entropy Alloys. The PMM group contributes to the Manutech-SLEIGHT Graduate School through the development of a specific knowledge about the metallurgy/mechanical/microstructure consequences induced by laser processing (laser beam melting, laser peening, laser surface texturing).

 

PUBLICATIONS
  • Jean-Philippe Colombier, Anton Rudenko, Elena Silaeva, Hao Zhang, Xxx Sedao, Emile Bévillon, Stéphanie Reynaud, Claire Maurice, Florent Pigeon, Florence Garrelie, Razvan Stoian, Mixing periodic topographies and structural patterns on silicon surfaces mediated by ultrafast photoexcited charge carriers, phys. Rev. Res. 2, 043080 (2020)
  • Bruzy, N., Coret, M., Huneau, B., Stainier, L., Denoual, C., Mondon, M., Kermouche, G. Real time imaging of strain fields induced by the ferrite-to-austenite transformation in high purity iron, Materials Today Communications 24, 2020, 101028. DOI: 10.1016/j.mtcomm.2020.101028.
  • S. Divin-Mariotti, P. Amieux, A. Pascale-Hamri, V. Auger, G. Kermouche, F. Valiorgue, S. Valette. Effects of micro-knurling and femtosecond laser micro texturing on aluminum long-term surface wettability, Applied Surface Science, 479, 2019,pp. 344-350. DOI: 10.1016/j.apsusc.2019.02.025
  • C. Courbon, A. Sova, F. Valiorgue, H. Pascal, J. Sijobert, G. Kermouche, P. Bertrand, J. Rech,. Near surface transformations of stainless steel cold spray and laser cladding deposits after turning and ball-burnishing, Surface and Coatings Technology, 371, 2019, pp 235-244. DOI: 10.1016/j.surfcoat.2019.01.092
  • S. Breumier, A. Villani, C. Maurice, M. Lévesque, G Kermouche, Effect of crystal orientation on indentation-induced residual stress field: Simulation and experimental validation, Materials & Design, 2019, 107659. DOI: 10.1016/j.matdes.2019.107659
  • Xxx Sedao, Anthony Abou Saleh, Anton Rudenko, Thierry Douillard, Claude Esnouf, Stephanie Reynaud, Claire Maurice, Florent Pigeon, Florence Garrelie, Jean-Philippe Colombier, Self-arranged periodic nanovoids by ultrafast laser-induced near-field enhancement, 2018, ACS Photonics, 5, 1418-1426.
More about the PMM team

PROCESSES IN DISPERSED AND MULTIPHASIC MEDIA - PDMM

The PDMM team works on physico-chemistry and dynamics of granular and particulate solids: image analysis, morphological characterizations and spatio-temporal models. These researches are applied to additive manufacturing (powder rheology), simulation of functional properties of solids in regards of morphology. PDMM's contribution to the Graduate School is mainly through the second research axis “Extract full information and meaning from surface imaging” with the objective to extract quantitative geometrical and morphometrical information, from correlative multi-mode image analysis techniques (photonic, electronic and RX), of tribologic surfaces in order to correlate them to tribologic measurements.
 
  • LGF_PDMM Pin-on-disk tribometer
    Pin-on-disk tribometer coupled with image acquisition © BOUCHOT-DESCARTES-GAVET-PINOLI_LTDS-LGF
    LGF_PDMM Pin-on-disk tribometer
  • LGF_PDMM_Third-body particles observed after a dry friction
    Third-body particles observed after a dry friction © BOUCHOT-DESCARTES-GAVET-PINOLI_LTDS-LGF
    LGF_PDMM_Third-body particles observed after a dry friction
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PUBLICATIONS
  • Solmaz Boroomandi Barati, Hélène Martin, Jean-Charles Pinoli, Stéphane Valette, Yann Gavet. Binarization of the gray scale images of droplets during dropwise condensation on textured surfaces. Fourteenth International Conference on Quality Control by Artificial Vision, 2019.
  • S Boroomandi Barati, Victor Rabiet, J-C Pinoli, S Valette, Y Gavet. Modeling and simulating the growth of ellipsoidal droplets during dropwise condensation on pillared surfaces. Applied Thermal Engineering, 148, p. 1370-1384, 2019.
  • Helene Martin, Solmaz Boroomandi Barati, Jean-Charles Pinoli, Stephane Valette, Yann Gavet. Segmentation of gray scale images of dropwise condensation on textured surfaces. International Journal of Computer and Information Engineering, 12(9), p. 753-731, 2018.
  • S Boroomandi Barati, Nicolas Pionnier, J-C Pinoli, Stéphane Valette, Yann Gavet. Investigation spatial distribution of droplets and the percentage of surface coverage during dropwise condensation. International Journal of Thermal Sciences, 124, p. 356-365, 2018.
More about the PDMM research group

SURFACE AND INTERFACE REACTIVITY AND FUNCTIONALISATION - SURF

The activities of the SURF group focus on Surface Reactivity on one hand, and Surface Functionalisation on the other hand. The Reactivity aspects include corrosion of materials in aqueous solutions, gas-solid surface reactions, high temperature corrosion and hydrogen embrittlement of materials, while the Functionalisation part of the group deals with surface processing to obtain particular sensory properties (visual and/or tactile) and to develop various sensors. On top of that, the SURF group has a unique expertise in the development of new AFM- and XPS-based methods, as well as optical methods, for surface analysis.
 
  • LGF_SURF Pre-oxidized Zy4 plate
    Pre-oxidized Zy4 plate © Gestin_LGF
    LGF_SURF Pre-oxidized Zy4 plate
  • LGF_SURF_Local detection of hydrogen at the surface of materials using Kelvin probe (SKPFM)
    Local detection of hydrogen at the surface of materials using Kelvin probe (SKPFM) © Tohme_LGF
    LGF_SURF_Local detection of hydrogen at the surface of materials using Kelvin probe (SKPFM)
_

PUBLICATIONS
  • J. Faucheu, B. Weiland, M. Juganaru-Mathieu, A. Witt, P.-H. Cornuault, Tactile aesthetics: Textures that we like or hate to touch, Acta Psychol. (Amst.). 201 (2019) 102950. https://doi.org/10.1016/j.actpsy.2019.102950.
  • Q. Cridling, R. Charriere, D. Jamon, M. Lenci, M. Pedeferri, D. Delafosse, Anodized titanium oxide thickness estimation with ellipsometry, reflectance spectra extrema positions and electronic imaging: importance of the interfaces electromagnetic phase-shift, Thin Solid Films. 709 (2020) 138181. https://doi.org/10.1016/j.tsf.2020.138181.
  • Y. Bleu, V. Barnier, F. Christien, F. Bourquard, A.-S. Loir, F. Garrelie, C. Donnet, Dynamics of carbon diffusion and segregation through nickel catalyst, investigated by in situ XPS, during growth of nitrogen doped graphene, Carbon. 155 (2019) 410–420. https://doi.org/10.1016/j.carbon.2019.08.084.
  • E. Tohme, V. Barnier, F. Christien, C. Bosch, K. Wolski, M. Zamanzade, SKPFM study of hydrogen in a two phase material. Experiments and modelling, Int. J. Hydrog. Energy. 44 (2019) 18597–18605. https://doi.org/10.1016/j.ijhydene.2019.05.177.
  • J.G.D. Preturlan, L. Vieille, S. Quiligotti, L. Favergeon, “Kinetics and mechanism of the dehydration of calcium sulfate dehydrate: a comprehensive approach for the dehydration of ionic hydrates under controlled temperature and water vapor pressure”, J. Phys. Chem. C 124 (2020) 26352-26367. https://doi.org/10.1021/acs.jpcc.0c09041
  • O. Kassem, M. Saadaoui, M. Rieu, J.-P. Viricelle, A novel approach to a fully inkjet printed SnO2-based gas sensor on a flexible foil, J. Mater. Chem. C. 7 (2019) 12343–12353. https://doi.org/10.1039/C9TC04170B.
More about the SURF research group: Mechanics, Physics, Interfaces
More about the SURF research group: PTSI